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  • Title: Tandem cyclization of α-cyano α-alkynyl aryl ketones induced by tert-butyl hydroperoxide and tetrabutylammonium iodide.
    Author: Wong YC, Tseng CT, Kao TT, Yeh YC, Shia KS.
    Journal: Org Lett; 2012 Dec 07; 14(23):6024-7. PubMed ID: 23190145.
    Abstract:
    The radical cascade protocol of the α-cyano α-TMS/aryl-capped alkynyl aryl ketones promoted by tert-butyl hydroperoxide under catalysis with tetrabutylammonium iodide in refluxing benzene has been developed, leading to the construction of a variety of highly functionalized [6,6,5] tricyclic frameworks in an efficient manner.
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