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  • Title: Synthesis of the C1-C21 domain of azaspiracids-1 and -3.
    Author: Zhang Z, Ding Y, Xu J, Chen Y, Forsyth CJ.
    Journal: Org Lett; 2013 May 17; 15(10):2338-41. PubMed ID: 23627769.
    Abstract:
    An efficient synthesis of the C1-C21 fragment of azaspiracids-1 and -3 is described. This features a Nozaki-Hiyama-Kishi reaction to couple the AB and CD ring precursors and formation of the THF-fused ABCD trioxadispiroketal system under thermodynamic conditions.
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