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  • Title: Palladium-catalysed aerobic oxidative Heck-type alkenylation of Csp3-H for pyrrole synthesis.
    Author: Meng L, Wu K, Liu C, Lei A.
    Journal: Chem Commun (Camb); 2013 Jul 04; 49(52):5853-5. PubMed ID: 23694954.
    Abstract:
    The first palladium-catalysed aerobic oxidative intramolecular alkenylation of Csp(3)-H bonds was described. The reaction conditions were mild and molecular oxygen was used as the terminal oxidant. Kinetic studies showed that the Csp(3)-H metallation step was a slow step.
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