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  • Title: Palladium-catalyzed Z-selective oxidative amination of ortho-substituted primary anilines with olefins under an open air atmosphere.
    Author: Mizuta Y, Yasuda K, Obora Y.
    Journal: J Org Chem; 2013 Jun 21; 78(12):6332-7. PubMed ID: 23731281.
    Abstract:
    The Pd-catalyzed oxidative amination of olefins with primary anilines has been achieved using molecular dioxygen as the sole oxidant. The use of ortho-substituted primary anilines such as ortho-toluidine was the key to the successful development of this reaction, providing the corresponding N-alkenyl substituted anilines in high yields with unusually high levels of Z-selectivity.
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