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  • Title: Matrix-free dynamic nuclear polarization enables solid-state NMR 13C-13C correlation spectroscopy of proteins at natural isotopic abundance.
    Author: Takahashi H, Hediger S, De Paëpe G.
    Journal: Chem Commun (Camb); 2013 Oct 21; 49(82):9479-81. PubMed ID: 24013616.
    Abstract:
    We introduce a general approach for dynamic nuclear polarization (DNP) enhanced solid-state NMR that overcomes the current problems in DNP experiments caused by the use of frozen solutions. Notably, we report for the first time a 2D (13)C-(13)C correlation spectrum of a protein without the use of isotopic labeling.
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