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  • Title: Bromodimethylsulfonium bromide/silver triflate-promoted glycosylations using glycosyl allenoates as donors.
    Author: Zhang Y, Wang P, Song N, Li M.
    Journal: Carbohydr Res; 2013 Nov 15; 381():101-11. PubMed ID: 24095942.
    Abstract:
    A series of novel glycosyl allenoates were prepared by condensions of hemiacetals with 3,3-dimethyl-4,5-allenoic acid. Their glycosylations with various alcohols under the promotion of bromodimethylsulfonium bromide/silver triflate smoothly proceeded to produce disaccharides. Studies reveal that allenic group is crucial for the efficient glylcosylation of glycosyl allenoate.
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