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  • Title: Iron-catalyzed oxidative direct α-C-H bond functionalization of cyclic ethers: selective C-O bond formation in the presence of a labile aldehyde group.
    Author: Barve BD, Wu YC, El-Shazly M, Korinek M, Cheng YB, Wang JJ, Chang FR.
    Journal: Org Lett; 2014 Apr 04; 16(7):1912-5. PubMed ID: 24635116.
    Abstract:
    Iron catalyzed oxidative coupling of salicylaldehydes with cyclic ethers proceeded through the direct α-C-H functionalization of ethers, forming the corresponding acetals in moderate to excellent yields. This is the first example of iron catalyzed selective C-O bond formation in the presence of a sensitive aldehyde moiety.
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