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  • Title: Palladium-catalyzed alkenylation of ketone enolates under mild conditions.
    Author: Grigalunas M, Ankner T, Norrby PO, Wiest O, Helquist P.
    Journal: Org Lett; 2014 Aug 01; 16(15):3970-3. PubMed ID: 25032503.
    Abstract:
    A protocol for a mild, catalytic, intermolecular alkenylation of ketone enolates has been developed using a Pd/Q-Phos catalyst. Efficient intermolecular coupling of a variety of ketones with alkenyl bromides was achieved with a slight excess of LiHMDS and temperatures down to 0 °C.
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