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  • Title: Diamonds are a spectroscopist's best friend: thin-film diamond mid-infrared waveguides for advanced chemical sensors/biosensors.
    Author: Wang X, Karlsson M, Forsberg P, Sieger M, Nikolajeff F, Österlund L, Mizaikoff B.
    Journal: Anal Chem; 2014 Aug 19; 86(16):8136-41. PubMed ID: 25032789.
    Abstract:
    The first combination of mid-infrared (MIR) tunable quantum cascade lasers (tQCLs) with thin-film diamond strip waveguides (DSWGs) suitable for advanced chemical sensing/biosensing is demonstrated. The sensing system is composed of thin diamond films grown on surface-passivated Si wafers via chemical vapor deposition (CVD) and microstructured using inductively coupled plasma (ICP) etching, serving as photonic waveguides for radiation emitted by a broadly tunable quantum cascade laser (tQCL) in the spectral regime of 5.78-6.35 μm (1570-1730 cm(-1)). The characterization of the free-standing diamond waveguides reveals excellent transmission properties across a broad MIR band. As a proof of concept, the detection of acetone in D2O via evanescent field absorption is demonstrated achieving a limit of detection (LOD) as low as 200 pL, which indicates a significant sensitivity improvement compared to conventional MIR slab/strip waveguides reported to date. Providing characteristic absorption features within the tuning range of the tQCL, studies using anisaldehyde as an analyte further corroborate the potential of tQCL-DSWG-based chemical sensors/biosensors.
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