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  • Title: Enantioselective total synthesis of the lignan (+)-linoxepin.
    Author: Tietze LF, Clerc J, Biller S, Duefert SC, Bischoff M.
    Journal: Chemistry; 2014 Dec 15; 20(51):17119-24. PubMed ID: 25345835.
    Abstract:
    An enantioselective total synthesis of the natural (+)-linoxepin (1) was accomplished in eleven steps from bromovanin (24). Key steps are a domino carbopalladation/ Mizoroki-Heck reaction with the formation of a pentacyclic system, an asymmetric hydroboration as well as an oxidative lactonization.
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