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  • Title: [The structure determination of a new alkaloid phlegmariuine-N by long-range two-dimensional and NOE difference NMR spectroscopy].
    Author: Miao ZC, Yang ZS, Feng R.
    Journal: Yao Xue Xue Bao; 1989; 24(2):114-7. PubMed ID: 2801132.
    Abstract:
    A new alkaloid, phlegmariuine-N, was isolated from Phlegmariurus fordii (Baker) Ching. In the present work, a technique of long-range 1H-1H and 13C-1H COSY in combination with NOE difference spectroscopy has been successfully used to connect the spin systems separated by quatermary carbons and heteroatom. Its structure has been elucidated as (I).
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