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  • Title: Simultaneous homonuclear and heteronuclear spin decoupling in magic-angle spinning solid-state NMR.
    Author: Mote KR, Madhu PK.
    Journal: Solid State Nucl Magn Reson; 2018; 90():7-12. PubMed ID: 29370958.
    Abstract:
    We show here an effective way of implementing simultaneously homonuclear and heteronuclear dipolar decoupling in magic-angle spinning (MAS) solid-state NMR. Whilst the homonuclear spin decoupling is applied on the 1H channel, heteronuclear spin decoupling is applied on the 13C channel. The 1H spins are observed in a windowed fashion in this case. The resultant 1H spectrum has higher resolution due to the attenuation of broadening arising from both homonuclear 1H-1H and heteronuclear 1H-13C interactions, with the latter normally leading to additional line broadening in 13C labelled samples. The experiments are performed at MAS frequencies of ca. 60 kHz.
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