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  • Title: Controlling the Amorphous and Crystalline State of Multinary Alloy Nanoparticles in An Ionic Liquid.
    Author: Garzón-Manjón A, Meyer H, Grochla D, Löffler T, Schuhmann W, Ludwig A, Scheu C.
    Journal: Nanomaterials (Basel); 2018 Nov 04; 8(11):. PubMed ID: 30400345.
    Abstract:
    Controlling the amorphous or crystalline state of multinary Cr-Mn-Fe-Co-Ni alloy nanoparticles with sizes in the range between ~1.7 nm and ~4.8 nm is achieved using three processing routes. Direct current sputtering from an alloy target in the ionic liquid 1-butyl-3-methylimidazolium bis(trifluoromethylsulfonyl)imide leads to amorphous nanoparticles as observed by high-resolution transmission electron microscopy. Crystalline nanoparticles can be achieved in situ in a transmission electron microscope by exposure to an electron beam, ex situ by heating in vacuum, or directly during synthesis by using a high-power impulse magnetron sputtering process. Growth of the nanoparticles with respect to the amorphous particles was observed. Furthermore, the crystal structure can be manipulated by the processing conditions. For example, a body-centered cubic structure is formed during in situ electron beam crystallization while longer ex situ annealing induces a face-centered cubic structure.
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