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  • Title: Geopolymerization enhanced hydrothermal synthesis of analcime from steel slag and CFBC fly ash and heavy metal adsorption on analcime.
    Author: Liu Z, Li L, Shao N, Hu T, Han L, Wang D.
    Journal: Environ Technol; 2020 Jun; 41(14):1753-1765. PubMed ID: 30403928.
    Abstract:
    This work is focused on crystal phase transition of solid wastes and functional application of crystal analcime in waste water purification, which provide a new environment-friendly route. In this paper, analcime was synthesized from steel slag and Circulating fluidized bed combustion (CFBC) fly ash (CFA) by hydrothermal method enhanced via geopolymerization (non-crystallized process). Then the analcimes were used for the removal of heavy metal ions (Pb2+, Cu2+) in aqueous solutions. Both the raw materials and products were characterized by XRF, XRD, FT-IR, SEM-EDS, and TEM. The results showed that non-crystallized process reduced the time of hydrothermal reaction and promoted the purity of analcime. The adsorption kinetics of analcime were all well fitted the pseudo-second-order model, and adsorption isotherms were well described by the Langmuir model. The maximum adsorption capacity of analcime for Pb2+ and Cu2+ were around 75.76, and 21.83 mg/g, respectively. The preference order observed for adsorption is Pb2+ > Cu2+.
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