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  • Title: Efficiency comparison of nylon-6-based solid-phase and stir bar sorptive extractors for carbamazepine extraction.
    Author: Alvani-Alamdari S, Jouyban A, Khoubnasabjafari M, Nokhodchi A, Rahimpour E.
    Journal: Bioanalysis; 2019 May; 11(9):899-911. PubMed ID: 31084189.
    Abstract:
    Aim: Two approaches based on molecularly imprinted polymers-stir bar sorptive extraction (MIP-SBSE) and -magnetic solid-phase extraction (MIP-MSPE) have been used for extraction of carbamazepine (CBZ) from serum samples. Methodology: In MSPE and SBSE, development was achieved by employing a polycaprolactam coating. The Cecil® chromatographic system equipped with a UV-Vis detector was used for analytical determination of CBZ. Results: The linearity of calibration curves was in the concentration ranges of 0.2-12 and 0.05-12 μg ml-1 for MIP-SBSE and MIP-MSPE, respectively. Conclusion: MIP-MSPE was selected in preference to MIP-SBSE since lower limits of detection were achievable using MIP-MSPE method. The CBZ-MIP-MSPE-HPLC-UV method was successfully applied to CBZ determination in real serum samples of patients receiving CBZ.
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