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  • Title: Calcium phosphate powder synthesis by out-of-phase pulsed sonoelectrochemistry.
    Author: Daltin AL, Beaufils S, Rouillon T, Millet P, Chopart JP.
    Journal: Ultrason Sonochem; 2019 Nov; 58():104662. PubMed ID: 31450292.
    Abstract:
    High aspect ratio calcium phosphate (CaP) nanorods were achieved by out-of-phase pulsed sonoelectrodeposition from electrolytic aqueous bath composed of calcium nitrate, ammonium dihydrogenophosphate and surfactant at pH of 4.9. The nature of CaP phases was determined by powder X-ray diffraction (PXRD), Fourier transform infrared spectroscopy (FTIR) and energy dispersive X-ray spectroscopy (EDX). The results reveal the predominantly presence of calcium deficient hydroxyapatite (CDHA). The transmission electron microscopy (TEM) analyzes highlighted that the nanorods are polycristalline and have an aspect ratio up to 30.
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