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  • Title: Recovery of metals from waste printed circuit boards by selective leaching combined with cyclone electrowinning process.
    Author: Guo X, Qin H, Tian Q, Li D.
    Journal: J Hazard Mater; 2020 Feb 15; 384():121355. PubMed ID: 31629590.
    Abstract:
    This paper provides a benign process that realized the metals separation and recovery from wPCBs in an efficient and low cost way. The chemical active order and potential-pH diagram of the metals enlightened us to apply stepwise leaching to selective separation of the metals from the wPCBs. The results indicated that the selective separation of Fe, Al, Zn; Sn and Cu can be achieved by the dilute sulfuric acid leaching, displacement leaching using copper sulphate and sulfuric acid leaching with air-oxidization, respectively. Under the optimal conditions, the leaching efficiency of Fe, Al, Zn, Sn and Cu were 92.59%, 90.51%, 89.73%, 1.44% and 0.82%, respectively, in the dilute sulfuric acid leaching. In the displacement leaching, the displacement efficiency of Sn was as high as 95.20%, with little Cu leached. The data of sulfuric acid leaching with air-oxidization experiments shows that the leaching efficiency of Cu reached 95.72%. In order to recover the Sn and Cu in the solutions, the hydrolysis precipitation and cyclone electrowinning were introduced. With these techniques, 92.75% Sn was precipitated and the smooth cathode copper (purity 99.98%) was obtained with the current efficiency was 94.96%. Moreover, the analysis of the mass distribution about the process demonstrated that the H+ and Cu2+ were consumed, but also produced in different procedure, that means the process is a simple and eco-friendly technology, not only due to its high recovery efficiency, but also high reagents recyclable.
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