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  • Title: Mesoporous silica supported orderly-spaced gold nanoparticles SERS-based sensor for pesticides detection in food.
    Author: Xu Y, Kutsanedzie FYH, Hassan M, Zhu J, Ahmad W, Li H, Chen Q.
    Journal: Food Chem; 2020 Jun 15; 315():126300. PubMed ID: 32018077.
    Abstract:
    In this study, a novel sensor fabricated with compactly arranged gold nanoparticles (AuNPs) templated from mesoporous silica film (MSF) via air-water interface has been confirmed as a promising surface-enhanced Raman scattering (SERS) substrate for detecting trace levels of 2,4-dichlorophenoxyacetic acid (2,4-D), pymetrozine and thiamethoxam. The densely arranged AuNPs@MSF had an average AuNPs size of 5.15 nm with small nanogaps (<2nm) between AuNPs, and exhibited a high SERS performance. SERS spectra of pesticides were collected after their adsorption on the AuNPs@MSF. The results showed that the concentration of 2,4-D, pymetrozine and thiamethoxam gave a good linear relationship with SERS intensity. Moreover, the designed SERS-based sensor (AuNPs@MSF) was stable for 3 months with ca. 3% relative standard deviation (RSD) and was applied successfully for the analysis of 2,4-D extraction from both environmental and food samples. The proposed SERS-based sensor was further validated by HPLC and showed satisfactory result (p > 0.05).
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