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  • Title: Lithium compound catalyzed deoxygenative hydroboration of primary, secondary and tertiary amides.
    Author: Bisai MK, Gour K, Das T, Vanka K, Sen SS.
    Journal: Dalton Trans; 2021 Feb 23; 50(7):2354-2358. PubMed ID: 33570073.
    Abstract:
    A selective and efficient route for the deoxygenative reduction of primary to tertiary amides to corresponding amines has been achieved with pinacolborane (HBpin) using simple and readily accessible 2,6-di-tert-butyl phenolate lithium·THF (1a) as a catalyst. Both experimental and DFT studies provide mechanistic insight.
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