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  • Title: Dissipation and residue of triadimefon in Rosa roxburghii.
    Author: Han L, Jiang Z, Zhang X, Wu X.
    Journal: Food Addit Contam Part A Chem Anal Control Expo Risk Assess; 2024 Aug; 41(8):914-922. PubMed ID: 38875459.
    Abstract:
    Rosa roxburghii (R. roxburghii) is a unique, edible, medicinal fruit rich in vitamin C found in Southwest China. Triadimefon (TDF) is a triazole fungicide that is widely used to control powdery mildew in R. roxburghii. To assess the safety of TDF in R. roxburghii, an LC-MS/MS method was developed for the simultaneous quantification of TDF and its major metabolite, triadimenol (TDN) in R. roxburghii. Both TDF and TDN showed high correlation coefficients (>0.999) for the solvent- and matrix-matched calibrations. The recovery rates of TDF and TDN in R. roxburghii ranged from 90.18% to 100.42%, with a relative standard deviation (RSD) of 1.25%-9.22%. The limit of quantification (LOQ) was 0.01 mg·kg-1. The half-life of TDF in R. roxburghii was between 2.74 and 3.07 days, with terminal residues ranging from < LOQ to 1.84 mg·kg-1. Recommended maximum residue limits (MRLs) and safe pre-harvest intervals (PHIs) for TDF in R. roxburghii were 0.5 mg·kg-1 and 21 days, respectively. This study provides essential data for TDF's safe and judicious use in R. roxburghii production.
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