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  • Title: High-performance liquid chromatographic determination of cephacetrile.
    Author: Mangia A, Silingardi S, Bortesi F, Grisanti G, Di Bitetto M.
    Journal: J Pharm Sci; 1979 May; 68(5):652-4. PubMed ID: 430511.
    Abstract:
    A rapid and accurate quantitative determination of cephacetrile in finished bulk and dosage forms is reported. The high-performance liquid chromatographic method is free of interference by acetyl hydrolysis products and synthesis by-products. The assay can be performed in about 15 min, affording less than 0.7% coefficients of variation within and between days. The chromatographic results are in good agreement with the microbiological assay requested by the "Code of Federal Regulations" for certification of cephacetrile sodium.
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