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  • Title: A high pressure liquid chromatographic method for the analysis of zearalenone in chicken blood.
    Author: Turner GV, Phillips TD, Heidelbaugh ND, Russell LH.
    Journal: J Environ Sci Health B; 1982; 17(4):297-309. PubMed ID: 6213701.
    Abstract:
    A high pressure liquid chromatographic (HPLC) method is described to determine zearalenone in chicken blood. Samples are extracted with acetonitrile, followed by a hexane cleanup procedure and extracted further with ethyl acetate. The analysis of zearalenone is by HPLC using a reverse phase radial compression separation system, an ultraviolet absorbance detector and a mobile phase of acetonitrile-water 60:40 (v/v). Recoveries of zearalenone in blood at levels of 50-200 ng/ml are in the range of 66.8-72.6%.
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