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  • Title: High resolution gas chromatographic analysis of nonpolar chlorinated hydrocarbons in human milk.
    Author: Bush B, Snow JT, Connor S.
    Journal: J Assoc Off Anal Chem; 1983 Mar; 66(2):248-55. PubMed ID: 6406422.
    Abstract:
    A gas chromatographic method is described for the analysis of human milk to determine polychlorinated biphenyls (PCBs) as 72 congeners plus p,p'-DDE, mirex, hexachlorobenzene, and octachlorostyrene. The detection limit for individual compounds is about 0.05 ng/g when 30 g milk is analyzed. Total PCBs can be estimated with a detection limit of 1-5 ng/mL milk. Analytical precision is better than +/- 10% for all compounds at 20-50 ng/mL whole milk.
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