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  • Title: Liquid chromatographic determination of nicarbazin in feeds and premixes.
    Author: Macy TD, Loh A.
    Journal: J Assoc Off Anal Chem; 1984; 67(6):1115-7. PubMed ID: 6520084.
    Abstract:
    A liquid chromatographic (LC) method has been developed for the determination of nicarbazin in premixes and poultry feed. Liquid chromatography of the 4,4'-dinitrocarbanilide (DNC) portion of nicarbazin is performed isocratically with a reverse phase octadecylsilica column and a UV detector set at 340 nm. The 2-hydroxy-4,6-dimethylpyrimidine (HDP) portion of nicarbazin is chromatographed isocratically with a reverse phase octylsilica column and a UV detector set at 305 nm. Nicarbazin concentration can be calculated by assaying both DNC and HDP, or by assaying DNC or HDP and assuming that nicarbazin is a 1:1 molar ratio of the two. Average recoveries of DNC and HDP added to poultry feed were 101% and 87%, respectively. This procedure provides an alternative to existing colorimetric procedures for determining nicarbazin in premixes and poultry feeds.
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