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Title: Separation and quantitation of perbenzoylated glucocerebroside and galactocerebroside by high-performance liquid chromatography. Author: Kaye EM, Ullman MD. Journal: Anal Biochem; 1984 May 01; 138(2):380-5. PubMed ID: 6742415. Abstract: Perbenzoylated gluco- and galactocerebrosides were separated and quantitated with a modification of existing HPLC methodology. A linear gradient of 0.9-18.4% dioxane in hexane was used to separate the derivatives on a pellicular silica column heated to 65 degrees C. The elevated temperature was the major modification that permitted the separation. This system was compared to a previously reported silica column/isopropanol in hexane system.[Abstract] [Full Text] [Related] [New Search]