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  • Title: [Gas chromatographic determination of thiocyanate in vegetable and animal foods and in human serum following paper chromatographic separation (author's transl)].
    Author: Thürkow B, Weuffen W.
    Journal: Pharmazie; 1981; 36(2):96-9. PubMed ID: 7232495.
    Abstract:
    Paper chromatographic separation of thiocyanate is the first step in determining non-bound thiocyanate in homogenized animal and vegetable foods and in human serum. The thiocyanate eluated from the paper chromatogram is brominated and then determined as cyanogen bromide using a gas chromatograph equipped with an electron-capture detector. Interfering substances (mainly ethanol-unprecipitable protein components, amino acids and cyanide from glycosidic precursors) are eliminated by this procedure.
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