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  • Title: High performance liquid chromatography of thiabendazole residues in banana citrus fruits.
    Author: Isshiki K, Tsumura S, Watanabe T.
    Journal: J Assoc Off Anal Chem; 1980 Jul; 63(4):747-9. PubMed ID: 7400086.
    Abstract:
    A simple high performance liquid chromatographic (HPLC) method for determining thiabendazole in fruits has been developed. Thiadazole is extracted with methanol and the extract is washed with n-hexane saturated with methanol. The determination is carried out by HPLC with fluorometric detection. LiChrosorb RP-8 is used as stationary phase and methanol-0.28% ammonia water (60+60) as mobile phase; alpha-methylindole is added as an internal standard. The limit of detection of this method is 0.1 microgram thiabendazole/g. Recoveries are more than 92%.
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