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  • Title: [The determination of toxic compounds with a dinitrophenol structure in the forensic chemical study of cadaveric material].
    Author: Shormanov VK, Fursova IA.
    Journal: Sud Med Ekspert; 1996; 39(3):40-4. PubMed ID: 8966736.
    Abstract:
    A method for forensic chemical assessment of dinitrophenol toxic compounds has been developed. Acetone was used as the isolating agent. The isolates were purified by extraction followed by adsorption in a column packed with silica gel. The analyzed substances are analyzed by chromogenic reactions, from UV and visible spectra in alkali and DMPA, and by thin-layer and high-pressure chromatography. The method allows the detection of 47-83% dinitrophenols in artificial mixtures with liver tissue (with 50 mg of analyzed substance per 100 g of the object). The detection minimum for this group of compounds is 0.5 to 1.0 mg per 100 g of cadaveric material.
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