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  • Title: Evaluation of allyldimethylsilyl ethers as steroid derivatives for gas chromatography-mass spectrometry.
    Author: Blair IA, Phillipou G.
    Journal: J Chromatogr Sci; 1977 Oct; 15(10):478-9. PubMed ID: 914966.
    Abstract:
    The preparation of allyldimethysilyl steroid ethers for the analysis of steroids by GC-MS has been studied in depth. The application of these derivatives is shown to be unsatisfactory due to competitive formation of allylsiloxane derivatives.
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