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  • Title: Synthetic study on a novel Asn-linked core structure: synthesis of a pentasaccharide alpha-D-Man-(1-->3)-[alpha-D-Man-(1-->6)]-beta-D-Man-(1-->4)- [beta-D-GlcNAc-(1-->60]-beta-D-GlcNAc-->OMp.
    Author: Guo ZW, Ito Y, Nakahara Y, Ogawa T.
    Journal: Carbohydr Res; 1998 Feb; 306(4):539-44. PubMed ID: 9679276.
    Abstract:
    Synthesis of a pentasaccharide alpha-D-Man-(1-->3)-[alpha-D-Man-(1-->6)] -beta-D-Man-(1-->4)-beta-D-GlcNac(1-->6)]beta-GlcNAc-->Omp (2) is described. A comparison between the 1H NMR data of 2 and those of a novel Asn-linked core structure 1 containing a new GlcNAc residue suggests an alpha-D-configuration for the new linkage.
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