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  • Title: Synthesis and purification of radioactive 6beta-iodomethyl-19-norcholest-5(10)-en-3beta-ol.
    Author: Scott KN, Couch MW, Mareci TH, Williams CM.
    Journal: Steroids; 1976 Aug; 28(2):295-303. PubMed ID: 973240.
    Abstract:
    A method for the synthesis and purification of 6beta-iodomethyl-19-norcholest-5(10)-ene-3beta-ol-131I of greater than 98 mole% chemical purity and greater than 99% radiochemical purity is presented. Carbon-13 and proton NMR were used to establish the identity and purity. Discrepancies in the characterization of this compound, previously published by two other research groups, are discussed.
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